Procedures ========== - Before you start making solutions in the Pchem lab, ensure that the Perkin Elmer Spectrum 400 FT-IR/FT-NIR Spectrometer is turned on (it should not be turned off) - Log into the :program:`Spectrum IR` software on the computer .. image:: images/software.jpg - In the Tabs on the bottom of the screen, you will be able to adjust several factors for your experiment such as: sample name, save location, instrument beam path, advanced settings, and basic instrument set-up - In this experiment, you will mainly be focusing on just sample name, save location, and basic instrument set-up to adjust a few parameters - It is also noted to adjust the parameters at the top of the page as well so that they reflect what you have included in the bottom (specifically *Sample ID*) .. image:: images/other_naming_settings.jpg Sample Naming ------------- - You can enter a name for your sample in both the *Auto-name* and *Auto-description* box after the *[nnn]* listed .. image:: images/naming_sample.jpg - Sometimes the auto-naming function does not work as you would like, so you may manually enter a name for the file up at the top of the page where it says ‘Sample ID’. Data Collection --------------- - Under *Auto-Save Options* you can chose where your files will save and the file format to export as .. image:: images/data_collection_settings.jpg Basic Instrument Settings ------------------------- - Here you can chose the wavelength range you wish to measure your samples within, the resolution, scan type, accumulations (how many scans), and units (absorbance, etc.) .. image:: images/instrument_setup_basic.jpg .. toctree:: Salt Plate Analysis Fixed Path Length Cell